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-
- From: harmon@Metaphor.COM
-
- > what is 'hash oil'?
-
- Its a thick black oil made from hash. The hash is heated and pressed to
- release the oil. (Same process used to make hash from marijuana, but carried
- to an extreme.) Its almost like a tar; very sticky, very thick.
-
- > how is it used?
-
- I've never seen it in the US, but When I lived in England, some 10 years ago,
- it was occasionally available. It came in two forms; sometimes it would be
- in a little plastic vial. Other times it would come in a piece of aluminum
- foil. From what I recall, the point was not to burn it, as that would burn
- off the active ingredients; but you wanted to inhale the vapor from it.
-
- The usual procedure was to get some heat resistant tube; the favorite was a
- the clear plastic tube that is the body of a bic disposable pen. Pull out the
- end cap, and pull out the ink/ballpoint thingy. Result: a clear plastic tube.
- Then, smear a small amount of the oil on a piece of aluminum foil. Hold the
- foil with pliers. With the oil on top, heat from beneath with a lighter.
- Hold the end of the tube above the patch of oil. As you begin to apply heat,
- suck like hell. The pliers (or something) are necessary because foil is
- an excellent conductor of heat, and you can burn yourself. It may take
- several heatings to use up all the oil from a smear. (You'll note this takes
- three hands!)
-
- For a nicer piece of equipment, take an old tablespoon. Bend the handle so
- that the handle bends away from the bowl, and then back so that it is pointing
- up away from the bowl. Attach same pen tube to the handle so that it points
- down into the bowl of the spoon. Smear oil into bowl of spoon, and heat
- spoon from bottom. (This only takes two hands.)
-
- Another technique, if you roll your own cigarettes, is to smear a streak of
- oil on a cigarette paper, and then roll a cigarette with this paper.
-
- ***************************** Article Separation ******************************
-
- From: harmon@Metaphor.COM
-
- I grew up in England, and when I was in high school (pun intended? ;-) there,
- all we could ever get was hash. For some peculiar reason, no one ever thought
- to use pipes. So we had to roll cigarettes with roll-your-own tobacco, and
- put crumbs of hash in them. Sometimes, to avoid the tobacco, we'd use
- disassembled clove cigarettes, or herbs like tarragon.
-
- If you've never used hash, (which I've never seen in the US,) it comes as a
- brown-green brick, which is VERY hard. You warm a corner over a lighter to
- soften it, and break crumbs off of it. You can't roll j's with this stuff; its
- solid. (Sometimes, good stuff is very dark in color, even black; this is
- usually very soft, and if squeezed, drops of hash oil may sweat out.)
-
- I don't seem to recall it being very common to find head shops where you could
- buy smoking equipment proper, but tobacco and rolling papers were very common.
- I don't think equipment was common, because I do remember a couple of pieces
- of homemade equipment; one friend of mine made a bong in his ceramics class. I
- made one with a thistle tube, cork, glass tubing, and erlenmeyer flask from
- a chemistry set of mine.
-
- ****************************** Article Separation *****************************
-
- From: cavasin@convex.com
-
- >> what is 'hash oil'?
- >Its a thick black oil made from hash. The hash is heated and pressed to
- >release the oil. (Same process used to make hash from marijuana, but carried
- >to an extreme.) Its almost like a tar; very sticky, very thick.
-
- No, make that very, Very, VERY sticky. Sticks to everything. stays under
- your fingernails for weeks after you've tried everything imaginable to get
- it out (and you try everything imaginable because the milligram or so that's
- stuck there is worth some money). It ruins clothes; the only thing that
- will take it off your skin or countertops is denatured alcohol or a similar
- solvent. The stickiest shit I have ever seen.
-
- >> how is it [hash oil] used?
-
- It turns up at dead shows occasionally. A "friend" had some that came from
- jamaica, which is where he assumes it was made.
-
- "friend" says the smoke is better than the vapor.
-
- >The usual procedure was to get some heat resistant tube; the favorite was a
- >the clear plastic tube that is the body of a bic disposable pen. Pull out the
- >end cap, and pull out the ink/ballpoint thingy. Result: a clear plastic tube.
- >Then, smear a small amount of the oil on a piece of aluminum foil. Hold the
- >foil with pliers. With the oil on top, heat from beneath with a lighter.
- >Hold the end of the tube above the patch of oil. As you begin to apply heat,
- >suck like hell. The pliers (or something) are necessary because foil is
- >an excellent conductor of heat, and you can burn yourself. It may take
- >several heatings to use up all the oil from a smear. (You'll note this takes
- >three hands!)
-
- Don't use a ballpoint pen unless you like to waste money (oil, same
- difference). This stuff costs a fortune--"friend" says $35/gram when you can
- get it. It's really not worth it at that price. Anyway, as far as heating it
- vs. warming it, "friend" says he's tried it both ways. Both ways it's real,
- real hard on your throat (worse than the harshest weed--almost as bad as that
- "black morrocan" lettuce O shit). It's a little harsher if you do the vapor
- thing. "friend" says seems to be more effective smoked, plus you waste less.
-
- best vapor method: put an old knife on a stove burner ("friend" used an
- electric stove; use a gas job at your own risk). let it get nice and hot (red
- hot isn't too hot, but of course you don't wanna deform the knife...). Get a
- paper towell tube or similar-size tube. GATHER EVERYONE AROUND CLOSE. use a
- real thin screwdriver or similar instrument to get a little dab of oil, stand
- ready with the tube, press the screwdriver against the hot blade and suck.
- don't take too much; it's got incredible expando properties. The stuff will
- smoke uncontrollably till it's gone, so make sure everyone gets in their suck
- without letting too much go to waste (it's good if everyone has their own
- tube).
-
- The aluminum foil method is okay, but "friend" thinks it's a little more
- wasteful. Eventually ya gotta throw that foil out.
-
- "friend" says best way to do it is to roll it with some herb (tobacco kills).
- Another good way to smoke it (according to friend) is to line a screened bowl
- with rolling paper or leaf and put a drop in there.
-
- However you do it, take SMALL hits. the shit is lethal on your lungs.
-
- Actually, now that friend thinks about it, the best way to do it is to put
- about 10 grams in a 13x7" brownie pan with your favorite brownie recipe. cut
- into ~1.25" squares. Eat one and have a wonderful night (sex is highly
- recommended). Eat two and become part of your favorite couch for 5 hours or
- so. Eat 5 or 6 and find out what heroin's like without having to mess with
- needles.
-
- Of course $350 is a hell of an expensive pan of brownies.
-
- >I always found that hash oil was much stonier than hash. (Whatever that
- >means.....) It gave me more of that feeling in my eyes of being in a smoky
- >room when I was stoned on plain hash or mj leaves.
-
- friend likes good hash better. Easier to smoke, tastes better. Right about
- the buzz tho. VERY intensly relaxing, almost paralyzing.
-
- >Of course, this was all long ago, and I don't do that sort of thing anymore....
-
- Of course, neither does friend.
- :^)
-
- A word of advice (from friend): BE CAREFUL when buying this shit. It's real,
- real easy to get ripped off, and doling out $35 for a gram of roofing tar is
- quite a bummer.
-
- Is hash oil mentioned in a faq? I'm too lazy to look. If it's not it should
- be.
-
- Oh, friend tells me to add one more thing: heating up the vial will make the
- stuff a lot easier to deal with (liquifies it). Also makes it more prone to
- spillage, so take great care when handling it in its liquid form. You can
- heat the vial with a lighter or put it on an electric stove burner.
-
- God, my friend is such a drug-craving unAmerican lowlife.:^)
-
- **************************** Article Separation ******************************
-
- From: kph@cisco.com (Kevin Paul Herbert)
- Date: 13 Sep 91 03:22:48 GMT
- Newsgroups: alt.drugs
- Subject: Re: How to purify THC from leaves?
-
- This comes from a friend of mine that doesn't have net access, so I won't be able to supply further details...
-
- 1. Run all leaf through a wire mesh sifter (such as a kitchen flour sifter)
- 2. Completely soak the leaf with ethyl or isopropyl alcohol for about 4 or 5 days.
- 3. Strain resultant product through silk (used for silk-screening)
- 4. Evaporate remainder by applying very low heat from kitchen stove
- Caution: be very careful - the product is *quite* flammable
- 5. After evaporating, there will be a remaining "goo". This is the hash oil.
-
- [It was noted in a followup that ispropyl alcohol is generally sold denatured,
- so that its vile to drink. The chemicals which denature it, however,
- *should* get evaporated by step 4, and further combusted when you smoke it.
- Therefore the effect of these chemicals *should* be minimal, but since I
- don't have the foggiest idea of what the chemicals actually are, use at your
- own risk -- Lamont]
-
- ****************************** Article Separation *************************
-
- From: goddard@cat55.cs.wisc.edu (Denis Goddard)
- Date: 15 Sep 91 20:33:53 GMT
- Newsgroups: alt.drugs
- Subject: Re: How to purify THC from leaves?
-
- In article <1991Sep13.032248.2685@csl.sri.com> kph@cisco.com (Kevin Paul Herbert) writes:
- >This comes from a friend of mine that doesn't have net access, so I won't be able to supply further details...
- >
- >1. Run all leaf through a wire mesh sifter (such as a kitchen flour sifter)
- >2. Completely soak the leaf with ethyl or isopropyl alcohol for about 4 or 5 days.
- >3. Strain resultant product through silk (used for silk-screening)
- >4. Evaporate remainder by applying very low heat from kitchen stove
- > Caution: be very careful - the product is *quite* flammable
- >5. After evaporating, there will be a remaining "goo". This is the hash oil.
- >
- >Kevin
-
- Use acetone instead of alcohol. THC is SUPER soluble in acetone - soak
- the ground-up leaves in acetone, then distill it off. best purity from
- any solvent I've ever tried. Next best choice is petroleum ether. Seriously,
- alcohols are too H2O - soluble for really good purity - lots of other
- nonpsychoactive stuff gets in the oil.
-
- P.S. once you've got the oil, it's REALLY sticky & hard to handle. mix with
- 2 parts powdered leaf to form good hash.
-
- you're welcome.
-
- ****************************** Article Separation *************************
-
- From: djh@osc.edu (David Heisterberg)
- Date: Thu, 19 Sep 1991 20:51:52 GMT
- Newsgroups: alt.drugs
- Subject: THC extraction
-
- Just for fun. Here are some exerpts from the Experimental section of
- a paper by Adams, Hunt, and Clark, JACS 62, 196 (1940).
-
- The hemp used in these experiments grew wild in Minnesota during
- the season of 1938. It was cut in August, after flowering had
- begun but before seed had "set" in the female tops. It was stored
- for six weeks in a room where a fan assured circulation of air in
- order to dry it completely. No molding occurred. The material
- was then beaten and shaken to remove the coarse stems which ammount-
- ed to about one-third of the total dry weight. The stems were dis-
- carded and the relatively fine material that remained was extracted
- with 95% ethanol [equivalent to Everclear] in the manner described
- below.
-
- Four 20-gallon (75-liter) crocks, each holding approximately 23 lb.
- (10 kg.) of material, were set up in series for countercurrent
- extraction. Each crock held approximately 61 liters of solvent of
- which about 41 liters were withdrawn at each transfer, the remain-
- der being retained by the hemp.
- ...
- The operations just described were carried out by Dr. John R. Matchett
- and his assistants in the Narcotics Laboratory of the Treasury
- Department, Washington, D.C. They kindly furnished us with a gener-
- ous supply of ethanol extract. [don't you wish you had connections
- like that?]
-
- The rest of the procedure involved removing ethanol and low boiling
- components under reduced pressure (about 30 mm) and gradually increased
- temperature (up to 200 C). The remaining oil was distilled at 3 mm,
- between 100-220 C. This crude oil (180-200 g) was disolved in petroleum
- ether (b.p. 30-60 C) and washed twice with water. The pet. ether was
- distilled off and the oil distilled at 2 mm, collecting the fraction
- boiling at 175-195 C, yielding 90-110 g of "purified red oil."
-
- So that's how the big boys did it back then. University of Illinois
- students and alums should note that the author Adams is none other than
- Roger Adams for whom the chem lab is named.
-
- At the time this paper was written it wasn't known just what the active
- ingredient in pot was. Cannabinol was the first compound identified in
- red oil, and cannabidiol had just recently been isolated. From the
- conclusion of the introduction:
-
- Red oil probably contains other products closely related to canna-
- binol or cannabidiol in structure, such as partially hydrogenated
- cannabinols, isomers of cannabidiol, or molecules like cannabidiol
- with less unsaturation. A large number of closely related compounds
- is possible. The active marihuana principle or principles may be
- among this group of substances. On the other hand, the possibility
- of the presence in red oil of a very potent active compound, entirely
- unrelated structurally to cannabinol or cannibidiol, is not excluded.
-
- Very soon after that is was determined that THC was the active principle.
- Roger Adams synthesized THC and several related compounds, some of which
- were several times more potent than THC. Roger Adams has a number of
- interesting papers, Joe Bob says "check it out."
-
- *************************** Article Separation ******************************
-
- From: lamontg@milton.u.washington.edu (Lamont Granquist)
- Date: Sun, 22 Sep 1991 04:05:13 GMT
- Newsgroups: alt.drugs
- Subject: Anon Post: Makin' Hash
-
- the following is an anonymous post which was forwarded to me by e-mail.
-
- You haven't seen this yet, even though its quoted.
-
- anonymous@somesite.somewhere sez:
- >The following details an attempt at making hash from MJ stems..
- >
- > On friday I took a handfull of stems I had left from a QP we got
- >about 6 months ago. The MJ itself was by far the worst I've ever
- >had.. I and 2 friends went through a half ounce without catching
- >a good buzz. But, I did keep the stems for some reason (Maybee
- >I thought it'd be nice to have a foot long stem for cleaning bowls..
- >Who knows..) Anyway.. This is what I did..
- >
- > Fraday.. Put one handfull of stems in a jar filled with rubbing
- >alcohol. (It's hard to get everclear when you're under 21)
- >
- > Saturday.. Decided not to waste a month just to find that the hash
- >was garbage, and did the following..
- > 1: Put jar of Stems/Alcohol in a pot of boiling water (Leaving
- > the top of the jar open and above the surface of the water)..
- > I let it boil for about 30 minutes then decided that this was
- > going a bit too slow..
- > 2: Strained Stems/Alcohol mix through 2 paper towels into a glass
- > pie plate. (I was going to use coffee filters, but couldn't
- > find any..)
- > 3: Put plate on stove and heated liquid until all of the rubbing
- > alcohol was gone. (This took aprox 45 minutes on Med-Low
- > heat.. The Alcohol was gone after about 30 minutes. <The mix
- > did not have an alcohol smell>)
- > 3.1 Caught one of the strangest buzzes ever while the mix
- > was evaporating..
- > 4: Scraped up what looked to be a dark-brown oil with a razor blade.
- > 5: Rolled the oil into a ball (This was no easy task.. The oil
- > seemed to liquify whenever I touched it..)
- > 6: Smoked the oil in a pipe.. One drag and I was buzzing. Another
- > and the pipe was clogged up.
- > 7: Used a match and pulled out the remaining oil.
- > 8: Used another match to set the remaining oil on fire.. It bubbled
- > and burnt on its own.
- >
- > Now for some questions about what happened..
- >
- > -Was it the Alcohol or MJ that was getting me stoned while I
- > was evaporating the mix?
- >
- > -Does rubbing alcohol leave behind any residue when it evaporates?
- >
- > -Does anyone out in net-land know of a better way to smoke the
- > oil? I'd rather not mix it with tobacco or MJ.
- >
- > -Someone on the net was saying to leave the MJ in alcohol for a month.
- > What I experienced today would tend to make me believe this
- > unnecessary. Did I lose alot of THC by boiling rather than waiting?
- >
- > -At what temperature does the THC itself start to break down?
- >
- > Thanks for any help you can offer.
- >
- >ANON
-
- ******************************* Article Separation **************************
-
- >
- > Awhile back on alt.drugs you posted about having references for how to
- > purify MJ into hash. I was thinking this would be really good to add
- > to the ftp site, along with the brownie recipies, etc.
-
- I don't personally own these books; I just saw them in a "books by phone"
- catalog along with a bunch of other books--you know, Knuth's _Art of
- Computer Programming_ volumes 1-3, Wirth's _Algorithms + Data Structures_...
-
- _Cannabis Alchemy_, by Gold, 1990
-
- _Great Book of Cannabis by Cherniak_, 1983
-
- _Marijuana Chemistry by Starks_, 1990
-
- I realize the above info is vague, but that's all the books by phone catalog
- listed.
-
- *************************** Article Separation *************************
-
- Anonymous writes:
-
- (1) to utilize leftover marijuana components - sticks, water leaves
- and the like - simply put it in a double boiler with some butter,
- and let it simmer for a few hours, then strain out the butter and
- put it into a plastic container in the fridge. It's easy to make
- several cubes' worth of pot butter in this fashion ... and half a
- cube is about the amount of margerine or butter one uses when one
- is making brownies. No vegetable material actually enters the mix,
- such that the resulting brownies are substantially safer to carry.
-
- i've spent maybe ten years playing with petroleum ether and sundry
- other solvents, and it's really a waste of time trying to make hash
- with small amounts of marijuana. the cost : effect ratio just isn't
- justifiable. whereas the same materials, when invested in pot butter,
- not only utilize _every_ component, but can get a whole room full of
- people high ... or keep you sane for a few weeks, one a day.
-
- (2) although this is not confirmed scientifically, i have read that it
- is believed that, when marijuana is burned, some of the CBN or CBD
- is converted to THC by the heating process. i have applied this to
- my own life by taking a handful of water leaves from said plant and
- microwaving them for about three minutes on defrost ( 40% duty cycle,
- which may not correspond to any other microwave oven manufacturer's
- energy usage profile ), blowing on them and stirring them around to
- evaporate the moisture this elicits, then nuking 'em for another
- similar period of time. this seems to make the resulting smoke just
- a bit stronger.
-
- It's really a shame that the Establishment doesn't apply itself to teaching
- people how to use drugs intelligently and creatively, since, clearly, such
- paths to competence and maturity exist. If I had known ten years ago what I
- have learned through much reading and thinking, I would have saved myself a
- lot of money, and, more importantly, a lot of grief and self-destructive
- behavior which I have, fortunately, survived.
-
- Please perpetuate this information as widely as possible, the better to teach
- people how to avoid addictive behavioral sequences while continuing to explore
- the realms of awareness in a mature and thoughtful manner.
-
- ************************* Article Separation *****************************
-
- anonymous2@anothersite.somewhere.else writes:
- >anonymous@somesite.someplace writes:
- >>(1) to utilize leftover marijuana components - sticks, water leaves
- >> and the like - simply put it in a double boiler with some butter,
- >> and let it simmer for a few hours, then strain out the butter and
- >> put it into a plastic container in the fridge. It's easy to make
- >> several cubes' worth of pot butter in this fashion ... and half a
- >> cube is about the amount of margerine or butter one uses when one
- >> is making brownies. No vegetable material actually enters the mix,
- >> such that the resulting brownies are substantially safer to carry.
- >>
- >> i've spent maybe ten years playing with petroleum ether and sundry
- >> other solvents, and it's really a waste of time trying to make hash
- >> with small amounts of marijuana. the cost : effect ratio just isn't
- >> justifiable. whereas the same materials, when invested in pot butter,
- >> not only utilize _every_ component, but can get a whole room full of
- >> people high ... or keep you sane for a few weeks, one a day.
- >
- >I have to disagree on the the 'waste of time' comment. In the past, I
- >have had (through an act of GOD) the great fortune of having multiple
- >ounces of green leafy material in my possession. As this material was
- >not quite suitable for smoking (taste reasons...), I sought out to
- >find a way to make use of it.
- >
- >The best method I ver used was really quite simple.
- >
- >First, I used a blender to turn the material into a fine powder. Then,
- >combine the material with enough acetone to completely cover it. Let the
- >mix soak for at least one or two days, covered and not near ANY flame
- >source. Then, strain the acetone into a crock-pot (slow cooker). It's
- >perfectly fine to have some of the finest ground material in the strained
- >acetone when done, as this helps the pseudo-hash burn nicely. Now, cook
- >the mixture on low heat until ALL the acetone has evaporated. Voila! You
- >now have the closest thing to the real mccoy, and it came from LEAF! If
- >you want to take it a step further, use a press to make small blocks. This
- >is more time consuming than it's worth, though.
- >
- >Works like a charm, and the result is quite pleasing, to say the least.
-
- ****************************** Article Separation ***************************
-
- EDITORIAL BY: lamontg@milton.u.washington.edu
-
- Also, there was much discussion of "double boilers". You use a double boiler
- whenever you are trying to heat, and evaporate volatile liquids. It should
- be reasonably obvious that this is necessary to boil off the [acetone|alcohol|
- isopropyl alcohol] which you would mix with the hash. A double boiler is
- simplely a large pot with water in it, which contains a smaller pot with the
- "pot" in it. The water in the large pot boils, heating the smaller pot but
- never exceeding the temperature of the boiling point of water. Thus, there is
- a much smaller risk of blowing yourself up.
-
- When dealing with flammable liquids like these solvents, proper ventalation
- is required, and flames are an absolutely contraindicated. There is a stupid
- text file running around the net on how to "make" Methamphetamine, which is
- actually a procedure for extracting psudoephedrine. One of the brilliant
- suggestions by the authors of this article was to evaporate by placing a
- solvent on a hot water heater. This is dumb. Real dumb. Particularly if
- you've got a gas hot water heater with a pilot light. (Can you say "Kaboom"
- boyz & girls? I knew you could...). Be a little careful.
-
- ******************************* Article Separation ************************
-
- FROM: Anonymous
-
- I don't ever touch marijuana anymore, but I had to comment on the correct
- method of smoking hash oil. When I was younger I had a girlfriend who lived
- in Calumet, in a little house on the edge of town. Across the road was
- an old tailings heap covered in long grass that waved in the wind. Anyway,
- she loved to drink ginger brandy and she loved to get high. She had some
- hash oil that summer and we smoked it together. Actually, I had more fun
- smoking it being high afterward. It was really too strong. But the smoking
- method was a kick, and it didn't waste any of the oil.
- We would sit at her kitchen table and heat a small, thin glass pipe
- with a crook in it, but no bowl (there had been a bowl once, but it had
- broken off, and it was not needed for the method) and heat the lower part
- WITH A PROPANE TORCH. Once the glass was glowing red, one of us would
- dip a wire loop into the hash oil and apply it to the inside of the lower
- extremity of the glass tube while the other person inhaled.
- The oil vaporized instantly, but some always precipitated on the inside
- of the pipe. After a few hits, we would 'cook' the pipe with the torch along
- its length to get this resin out.
- I maintain that this method, as opposed to others described, is truly
- efficient and easy--AND YOU GET TO WAVE A FLAMING PROPANE TORCH AROUND
- WHILE GETTING UNREASONABLY HIGH!!
-
- [Disclaimer: If you need a disclaimer to point out the potential danger of
- doing this, then you're too dumb to live and we can just think of it as
- natural selection in action -- Lamont]
-
- ***************************** Article Separation ******************************
-
- From: fiend@sideways.welly.gen.nz (Fiend)
- Date: Tue, 15 Oct 91 14:24:01 Y
- Newsgroups: alt.drugs
- Subject: HASH EXPERIMENTATION
-
- I read with interest a compilation of older net messages regarding the usage of
- hash oil and hash block.
-